《分析测试技术与仪器》 2022 年（共 4 期，按页码顺序）总目录

*大型仪器维护与维修

RFDA-HTVP-1750C 高温动态弹性模量与阻尼分析仪的维护与常见问题探讨 ······························· ··························································································余建新，焦 阳，王晓鹏 （ 1 ）

HydraⅡ C 自动测汞仪两例故障分析及排除 ··· 王 东，孙春晓，王 伟，马 玲，吕新明，徐新忠 （2 2 8）

原子吸收分光光度计石墨炉原子化法故障排除及原因分析 ······················································ ······················································余政军，尹小红，李海林，杨 柳，毕晶秀，傅志强 （3 0 8）

Isoprime 100稳定性同位素比质谱仪故障分析及排除 ··························· 谷淑波，徐 毅，金 敏 （4 7 3）

EVO MA 15钨灯丝扫描电子显微镜的日常维护 ············································· 陈新芳，周静韵 （4 8 0）

*综述

氮川三乙酸的样品前处理和检测方法研究进展 ··································· 程嘉雯，马继平，田 永 （ 8 ）

离子色谱法在中药化学成分分析中的应用进展 ····································································· ····················································· 颉东妹，魏晗婷，王宁丽，刘建飞，郭 玫，邸多隆 （1 7 9）

调节三高类中成药和保健食品中非法添加化学药物及其检测研究进展 ····· 李文斌，张 萍，徐 莹 （1 8 8）

光谱法水质监测仪器和方法国内专利状况分析 ····································································· ····················································· 常玺凤，虞功亮，韩璐璐，王 涛，时安琪，乔之怡 （3 1 2）

基于CiteSpace的实验队伍研究热点和趋势 ··················································· 岳 琦，王 晋 （3 2 0）

生物质炭的制备及其在吸附中的应用 ··································· 丁娜娜，梁锦华，乌 兰，张海霞 （3 6 3）

基质辅助激光解析电离飞行时间质谱分析合成聚合物样品制备的研究进展 ······················· 代莉莉 （3 7 5）

毛细管电泳在生物大分子分析中的应用研究进展 ···················· 彭 乐，程佳伟，李淑楠，李文龙 （3 8 4）

*浙江省大型科研仪器开放共享平台－国产科研仪器研发与应用专栏

智能数字聚合酶链式反应系统的开发与应用验证 ···················· 尚君鹏，贺晓伟，方秋雨，牟 颖 （ 18 ）

数智物联岩石力学背包实验室的自主创新 ····························· 伍 劼，伍法权，乔 磊，张 芳 （ 24 ）

二维核磁共振技术解析盐酸帕罗西汀 ······································································· 毛侦军 （ 31 ）

基于波数校准下傅里叶红外气体分析仪模型传递的研究 ························································· ············································ 查丽霞，周新奇，陈 磊，尚庆贺，王 兵，李康康，周志明 （ 37 ）

高效液相色谱法快速测定参芪降糖胶囊中人参皂苷的含量 ································ 林灵超，黄 燕 （ 45 ）

顶空-气相色谱法测定水中三氯甲烷和四氯化碳方法的改进 ··················· 王琼琼，黄翌磊，李俊珂 （ 51 ）

浙江省国产科研仪器发展现状分析及对策 ····························· 陈 盼，陈 宁，亓云涛，赵志娟 （ 57 ）

加快推进国产科研仪器“进口替代”的思考 ·············· 袁 勇，付国春，戴灵豪，谢晓笑，张燕勤 （ 62 ）

*分析测试新成果

固相萃取-气相色谱-质谱法测定3种中药材中 18种多环芳烃 ················ 李文斌，池艳艳，程 菲 （ 68 ）

固体进样-石墨炉原子吸收法测定农产品中重金属元素含量 ······· 莫 辉，游晓莹，潘小平，池巧东 （ 80 ）

长庆油田石油磺酸盐中活性组分识别 ················································································· ········································· 徐飞艳，王永宏，张 英，冯春艳，李文宏，王 帅，郭 勇 （ 88 ）

响应面优化微波辅助Fenton法降解活性艳蓝KN-R ······························································· ········································· 林晓森，薛祥航，董慧敏，方淑兵，丁美琪，赖紫宣，陈毅挺 （1 4 4）

高温比热容测试常见问题及误差分析 ······················· 焦 阳，刘春凤，王晓鹏，孙昭媛，余建新 （1 5 3）

Co3O4/CeO2复合电极材料的制备与超级电容器电化学性能研究 ························· 唐明华，王 颖 （4 0 0）

超高效合相色谱法测定缬沙坦原料药中R-缬沙坦 ·································································· ····················································· 丁建营，刘发贵，王 花，刘思光，李铁健，张贵民 （4 0 5）

高效液相色谱法测定磷酸三甲苯酯中游离甲酚的含量 ·························· 王世平，牛静静，杜亚珍 （4 1 1）

金银花绿原酸提取方法研究 ··································· 李 辉，逯桃桃，陈 佳，赵 亮，邱洪灯 （4 1 6）

*分析测试经验介绍

QuEChERS-超高效液相色谱串联质谱法快速测定婴幼儿奶粉中5种黄曲霉毒素含量 ····················· ····························· 王小乔，许晓辉，张虹艳，冯 翀，吴福祥，潘秀丽，李 赟，李晨曦 （ 96 ）

高效液相色谱法测定镍镀液中的糖精钠和苯亚磺酸钠 ···························································· ········································· 王 焱，董玉坤，李瑞基，冯建华，郭 勇，卢晓锋，李亦婧 （1 0 3）

微波消解-电感耦合等离子体质谱法测定血液中 30 种微量元素 ················································· ············································································· 火 婷，毛宝宏，李亚丽，任 伟 （1 9 8）

气相色谱法测定烟草浸膏中的烟碱 ·············· 肯生叶，段 勤，苏丹丹，杨 屹，田飞宇，杨雪燕 （2 0 5）

玻璃类注射剂用药包材内表面耐受性测试研究 ··············································· 聂 蕾，范 旭 （2 1 0）

上游水库水体中氨氮、亚硝酸盐氮、硝酸盐氮、总氮的测定和关系探究 ···························· 赵文斌 （2 2 2）

气相色谱柱对多溴联苯醚分析的影响 ··································· 张 炜，冯 灏，张 冰，杨永坛 （3 2 7）

基于CIRAS-3光合仪的CO2响应曲线测定 ··············· 饶心雨，杨翠珍，李永平，李自文，宋志姣 （3 3 4）

基于气相色谱-质谱和网络药理学探讨紫斑罂粟壳挥发油镇咳祛痰平喘的作用机制 ······················· ····· 宋小兰，王丽萍，赵宁娟，李建慧，杨 璐，王 诺，康文利，王小忠，张 伟，武全香 （3 4 3）

高效液相色谱-二极管阵列检测器法测定复方丹参片中12种成分及掺伪鉴别 ········ 范可青，凌 霞 （3 5 3）

电感耦合等离子体发射光谱法测定铝合金中的多种金属元素 ········································· 孙永放 （3 5 8）

微波消解-电感耦合等离子体原子发射光谱法测定钼铁合金中的钼含量 ······································ ····················································· 赵炳建，赵浩年，赵 越，史 琦，李小林，袁 辉 （4 2 2）

电感耦合等离子体质谱法测定地龙药材中铅、砷、汞、镉、铜元素的残留量 ·································· ································································· 马 彧，李正刚，曲涵婷，赵 艳，王路宏 （4 2 7）

冷冻扫描电子显微镜冷冻断裂法在生物样品观察中的应用 ······················································ ····················································· 黄克让，王 珍，陈 蕾，崔凤展，彭潔莹，张 敏 （4 3 3）

超高效液相色谱-串联质谱法同时测定化妆品中50种非法添加药物 ···················· 廖文榕，黄健浩 （4 3 9）

电感耦合等离子体发射光谱法测定三氯化钌溶液中杂质元素含量 ············································· ································································· 张玉德，刘荣正，罗 雄，崇 彪，白文刚 （4 5 1）

偏光显微镜与X射线衍射仪联用技术测定化妆品中石棉含量 ···· 张 雷，苏粉良，王海瑞，胡积东 （4 5 7）

粉末X射线衍射法测定消咳宁片中碳酸钙含量 ······················ 张建平，孙倩男，周雪梅，王 栋 （4 6 3）

树脂包埋在透射电子显微镜测试中的应用 ········································· 王小曼，梁 正，卢 思 （4 6 9）

*大型仪器科学管理

中国科学院检验检测机构资质认定概况 ························································ 申孟芝，张红松 （1 0 8）

质谱平台的运行管理和开放共享 ············································································· 卢巧梅 （1 5 9）

大型科学仪器专业技术培训促进使用效益提升的思考 ···························································· ········································· 张丽娜，杨 娟，吴爱华，包郁明，巫祥云，孙莹璐，韩玉刚 （1 6 3）

*浙江省大型科研仪器开放共享平台–电子显微镜专栏

<113>c晶带轴下Ba(B'1/3B″2/3)O3钙钛矿B位 1∶2 有序结构的透射电镜表征 ······························ ············································································· 马翩翩，刘观福，乔 茵，徐人豪 （1 1 3）

钐钴合金等温时效过程中胞状组织结构的透射电镜表征 ························································· ································································· 吴海辰，刘 壮，王新明，陈国新，卢焕明 （1 1 8）

导电环氧树脂消除扫描电子显微镜图像荷电问题的原理与实践 ················································ ·············································································· 彭 宇，张之恒，安 婷，钱匡亮（1 2 5）

扫描电子显微镜在缓释微球制剂表征中的应用进展 ················· 陈 超，樊海丽，蔡志威，张传杰 （1 3 2）

pH调控水热法合成BiVO4及其可见光催化降解甲基橙 ··········· 秦玉娇，蒋琦锐，张智芝，王林霞 （1 3 9）

纯锌中变形孪晶界精细结构的透射电子显微镜表征 ······························································· ····················································· 吴海辰，陈国新，于海涛，沈圣成，梁 芮，卢焕明 （2 4 7）

扫描电子显微镜和能谱分析高性能热塑性板材 ····································································· ········································· 郑 娜，徐 丽，沈素丹，贺 静，房尔园，浦 群，介素云 （2 5 4）

扫描电子显微镜-能谱联用在鉴别药包材上的应用 ······························· 蔡志威，梁键谋，陈 超 （2 6 0）

新氢压缩机活塞杆断裂原因分析 ····· 姚懿容，蒋蓉蓉，段北晨，管建敏，熊发浩，李 明，卢焕明 （2 6 7）

扫描电子显微镜在鹌鹑蛋壳表征中的应用 ····················································· 郑 希，戎念杭 （2 7 3）

扫描透射电子显微镜技术及其在中药研究中的应用 ····················································· 王月霞 （2 8 0）

扫描电子显微镜运行和管理的实践与探索 ····························· 何益超，盛国栋，陈朝贵，王林霞 （2 8 9）

*浙江省大型科研仪器开放共享平台-大型科研仪器开放共享管理研究专栏

高校大型科研仪器开放共享运行机制探究 ········································· 亓文涛，陈 盼，高 然 （1 6 7）

高校和科研院所分析测试中心质量管理体系重要性和建设举措探究 ·········································· ································································· 张 丽，李子厚，陈 波，贾亚茹，戚淑燕 （1 7 3）

*研究报告

聚（异丙基甲基丙烯酰胺）@聚（N-异丙基丙烯酰胺）中空微凝胶合成过程的形态学表征 ··················· ············································································· 郭宏博，白 露，胡西学，孙 迪 （2 3 3）

脱氧核糖核酸变性和损伤的原子力显微镜液相观察 ······························································· ··········································骆芸尔，高 珊，伊 艺，陆 奕，郑 寓，王艳伟，潘海鸥 （2 4 1）

*分析测试新方法

电感耦合等离子体质谱法测定新型抗菌不锈钢在生理盐水和磷酸盐缓冲液中的镓溶出量 ··············· ························································································· 于英杰，李 辉，张重远 （2 9 3）

无衍生化-气相色谱法测定药用胶塞提取液中硬脂酸和棕榈酸 ·················································· ································································· 余秋玲，马 艳，谢 威，杨 倩，龙 梅 （2 9 9）

离子色谱法快速测定氯化钾中微量溴离子和硫酸根离子 ··································· 金 珍，闫春辉 （3 0 4）

*大型仪器功能开发

物理吸附系统的改造及其测试 ···················· 陈佩丽，王树加，陈凯悦，陈晓丽，付 娟，苏秋成 （3 9 2）